#1
Kleine bump, hebben meer mensen dit middel al geprobeerd? Ben er zelf erg benieuwd naar, ook i.v.m. normale DMT ![:)]()
Helemaal mee eens. Maar puur om te testen wou ik zien of ik lui kon zijn en dit spul gewoon online scoren. Maar sowieso is er iets aan zelf plantjes groeien / plantmateriaal extraheren etc dat de ervaring ermee superieur maaktJe eigen DMT extraheren is niet zo moeilijk hoor. Dan krijg je zeker wel een breakthrough, en het plantmateriaal kun je gewoon online kopen, en in sommige smartshops (wel heel duur vaak)![]()
+1.Kleine bump, hebben meer mensen dit middel al geprobeerd? Ben er zelf erg benieuwd naar, ook i.v.m. normale DMT![]()
Deprotection of Tert-Butyloxycarbonyl (N-BOC) Groups Using a Microwave
Do you have a protected amine research chemical that can't be ingested on its own due to amine protection? If yes, then this is the guide for you! A fair warning that this method produces non-toxic byproducts such as sodium carbonate and/or unreacted hydrocarbons which may be toxic. There are ways to get rid of these through purification through acetone. This method may be in the next guide.
Now onto the good stuff:
Firstly, obtain either 95% everclear or anhydrous isopropyl alcohol (preferred due to ease of drying). Dissolve 0.334 millimolar equivalent of your protected amine into 2ml of your solvent of choice in a 10ml borosilicate beaker. If you can't get it to dissolve you can heat it mildly though be warned you may need to add more solvent to get back to 2ml due to evaporation. Add 29mg (0.334mmol/equimolar quantities) of baking soda to the solution and allow it to dissolve (arm and hammer is best because it contains no additives and is only pure sodium bicarbonate).
Next add your beaker into the microwave reactor (any microwave works for this though you'll have to do some calculations based on your microwaves power in wattage). Place some sort of covering over top of the beaker (saran wrap is good). Set that bitch to 300 watts and cook for 5 minutes making sure to observe the process in the rare case of fires. After, allow the alcohol to evaporate in an open dish.
That's it! You have a safe product to vaporize and the expected yield is an astonishing 95%!
Notes on the microwave process:
You need a total of 300 watts output power at 2450 MHz which is standard frequency for microwaves- though anything around this works well. The power settings on microwaves are percentages of the expected output power. Level three being 30% as seen in the guide which is 1000*0.3=300. If your microwave is a different wattage- do whatever percentage is closest to 300 watts.
Notes on the molar equivalencies:
I'm guessing N-BOC-DMT's formula is C17H24N2O2 or SMILES CN(CCC1=CNC2=C1C=CC=C2)CC(=O)OC(C)(C)C and thusly has a molar mass of 288.38466 g/mol, though I'm unsure of this because I couldn't find it online. Either way the molar mass of your compound can be put into this calculator https://calculator-online.net/moles-to-grams-calculator/ all you have to do is add the g/mol mass and the number 0.334 in the moles area when calculating mass in grams. Make sure to put the moles as mmol and not mol!
Citation: https://www.sciencedirect.com/science/article/abs/pii/S0040403908023502
Enjoy!
-Trimipramine
For anyone wondering, u/straightfromLysurgia provided the outline amounts for those of us that suck at basic chemistry and I refined it with my experiment:
Assuming NB-DMTs M is 288g/mol (from what I've gathered online, should be) we are working with 3.472mmol (1G) of NB-DMT.
The method I am referring to calls for adding 21mL of solvent, Isopropyl was my choice due to ease of access but Ever clear is fine too.
The amount of sodium bicarbonate is the same as NB-DMT, so 3.472mmol (311mg).
Dissolve your NBoCDMT into solvent, dissolve sodium bicarbonate into solvent, cover with saran wrap and blast on microwave for 5 minutes at 300w.
Let solvent evaporate for 12h. And done!
Is het een beetje te roken/vapen en hoe smaakt het? Is het echt verschrikkelijke chemische lucht of valt het mee?Nboc-dmt inmiddels gekocht, een paar testruns gedaan, maar nog geen breakthrough met 70mg...wel mooie cev.
Volgende poging met 100mg. Hopelijk krijg ik alles binnen, 😁.
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